Elastic deformation of non-uniform polymer crusts formed by droplet evaporation

D. A. Head

Department of Applied Physics, Tokyo University, Tokyo, JAPAN.


Crust formation of an evaporating polymer solution is an  important technical process for micron-scale manufacturing processes.  For a droplet on a wetting surface, the crust takes a cap-shape that  elastically deforms under the osmotic pressure arising from  continuing evaporation through the porous solid. A variety of shapes  have been observed in experiments, including so-called "craters" and  "mexican hats" - however, it is not clear  for what parameters (crust  thickness, contact angle etc.) each shape arises. We have investigated this phenomenon using quasi-static simulations and have  constructed a "phase diagram" of contact angle versus crust thickness  to show where each shape arises. Our protocol is pressure-controlled  rather than volume-controlled, both to simplify the numerical  procedure and to allow us to draw on a significant literature of  elastic spherical caps. We have also looked into the effects of non- uniform shell thickness, since the nature of droplet evaporation  suggests the crust formed will be thicker near the contact line than  the apex. In parallel with these numerical studies, we will also  present some approximate theoretical calculations that incorporate  non-linear strains. This is crucial, as the various shapes only  emerge under non-linear deformation; linear strains always produce  qualitatively similar results. Some recent results on symmetry- breaking deformations will also be given